(4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

Base Information

Chemical Name:(4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane
CAS No.:1402010-10-9
Molecular Formula:C₃₀H₄₁BO₃
Molecular Weight:460.465
Hs Code.:

Synonyms:(4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

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Chemical Property of (4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

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Technology Process of (4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

There total 1 articles about (4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1402010-09-6
(4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

: 100-51-6,185532-71-2
benzyl alcohol

: 1402010-10-9
(4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

Guidance literature:: benzyl alcohol; With n-butyllithium; In tetrahydrofuran; at -78 ℃;

With dimethyl sulfoxide; In tetrahydrofuran; at -78 - 20 ℃; for 18h;

(4S,5S)-2-((R)-1-chloro-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane; In tetrahydrofuran; at -78 - 20 ℃; for 36h; stereospecific reaction;
DOI:10.1021/ja307861n

Reference yield: 96.0%

: 75-09-2
dichloromethane

: 1402010-10-9
(4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane

: (4S,5S)-2-[(1R,2R)-2-(benzyloxy)-1-chloro-4-phenylbutyl]-4,5-dicyclohexyl-1,3,2-dioxaborolane

Guidance literature:: dichloromethane; (4S,5S)-2-((S)-1-(benzyloxy)-3-phenylpropyl)-4,5-dicyclohexyl-1,3,2-dioxaborolane; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -40 ℃; for 0.166667h;

With zinc(II) chloride; In tetrahydrofuran; hexane; at -40 - 20 ℃; for 2h;
DOI:10.1021/acs.orglett.1c03164