methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate

Base Information

• Chemical Name: methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate
• CAS No.: 160628-35-3
• Molecular Formula: C₂₄H₃₃NO₄Si₂
• Molecular Weight: 455.701

Synonyms:methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate

Chemical Property of methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate

Chemical Property:

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Technology Process of methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate

There total 2 articles about methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Methyl glyoxylate (922-68-9) + 1,4-diphenyl-3-(trimethylsilyl)azetidin-2-one → methyl hydroxy<2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>acetate + methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate (160628-35-3)

Guidance literature:

With chloro-trimethyl-silane; lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 15 min; 2.) THF, -78 deg C, 15 min; 3.) THF, r.t., 1 h;

DOI:10.1002/hlca.19940770808

Reference yield:

chloro-trimethyl-silane (75-77-4) + Methyl glyoxylate (922-68-9) + 1,4-diphenyl-3-(trimethylsilyl)azetidin-2-one → methyl hydroxy<2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>acetate + methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate (160628-35-3)

Guidance literature:

With lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C, 15 min; 2.) THF, -78 deg C, 15 min; 3.) THF, r.t., 1 h;

DOI:10.1002/hlca.19940770808

Reference yield: 78.0%

methyl <2-oxo-1,4-diphenyl-3-(trimethylsilyl)azetidin-3-yl>(trimethylsilyloxy)acetate (160628-35-3) → (E)-methyl (2-oxo-1,4-diphenylazetidin-3-ylidene)acetate

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 2h;

DOI:10.1002/hlca.19940770808

upstream raw materials:

chloro-trimethyl-silane

Methyl glyoxylate

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