2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline

Base Information

Chemical Name:2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline
CAS No.:908123-58-0
Molecular Formula:C₁₉H₂₆N₂O₄
Molecular Weight:346.426
Hs Code.:

Synonyms:2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline

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Chemical Property of 2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline

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Technology Process of 2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline

There total 5 articles about 2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 2-(N-ethoxycarbonylaminomethyl)-N-ethoxycarbonylaniline

: 107-05-1
3-chloroprop-1-ene

: 908123-58-0
2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 90 ℃; for 6h;
DOI:10.1055/s-2006-942360

Reference yield:

: 908123-56-8
N-benzyl-N-ethoxycarbonyl-2-nitrobenzylamine

: 908123-58-0
2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / Pd/C / methanol / atmospheric pressure

2: 67 percent / Et₃N / CH₂Cl₂ / 24 h / 20 °C

3: 64 percent / NaH / dimethylformamide / 6 h / 90 °C

With hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-942360

Reference yield:

: 95982-61-9
o-nitro-N-benzyl(benzylamine)

: 908123-58-0
2-(N'-allyl-N'-ethoxycarbonylaminomethyl)-N-allyl-N-ethoxycarbonylaniline

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: 95 percent / H₂ / Pd/C / methanol / atmospheric pressure

3: 67 percent / Et₃N / CH₂Cl₂ / 24 h / 20 °C

4: 64 percent / NaH / dimethylformamide / 6 h / 90 °C

With hydrogen; sodium hydride; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-942360