ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate

Base Information

Chemical Name:ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate
CAS No.:479480-54-1
Molecular Formula:C₁₅H₂₇F₂NO₃S
Molecular Weight:339.447
Hs Code.:

Synonyms:ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate

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Chemical Property of ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate

Chemical Property:

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Technology Process of ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate

There total 2 articles about ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 667-27-6
Ethyl bromodifluoroacetate

: 336105-28-3
(R_S,E)-N-(cyclohexylmethylene)-2-methylpropane-2-sulfinamide

: 479480-54-1
ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate

: ethyl (3S)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate

Guidance literature:: Ethyl bromodifluoroacetate; With zinc; In tetrahydrofuran;

(R_S,E)-N-(cyclohexylmethylene)-2-methylpropane-2-sulfinamide; In tetrahydrofuran; at 20 ℃; for 18h; Further stages.;
DOI:10.1021/jo0259313

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 479480-54-1
ethyl (3R)-3-[(tert-butylsulfinyl)amino]-3-cyclohexyl-2,2-difluoropropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: CuSO₄; molecular sieves / CH₂Cl₂

2.1: Zn / tetrahydrofuran

2.2: tetrahydrofuran / 18 h / 20 °C

With molecular sieve; copper(II) sulfate; zinc; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo0259313