C₁₅H₁₄ClN₃O

Base Information

Chemical Name:C₁₅H₁₄ClN₃O
CAS No.:1365627-76-4
Molecular Formula:C₁₅H₁₄ClN₃O
Molecular Weight:287.749
Hs Code.:

C<sub>15</sub>H<sub>14</sub>ClN<sub>3</sub>O

Synonyms:C₁₅H₁₄ClN₃O

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Chemical Property of C₁₅H₁₄ClN₃O

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Technology Process of C₁₅H₁₄ClN₃O

There total 1 articles about C₁₅H₁₄ClN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1365627-74-2
C₁₃H₁₀ClN₃O

: 74-88-4
methyl iodide

: 1365627-76-4
C₁₅H₁₄ClN₃O

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 0 - 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2012.01.015

Reference yield: 34.0%

: 1365627-76-4
C₁₅H₁₄ClN₃O

: 109384-19-2
t-butyl 4-hydroxy piperidine-1-carboxylate

: 1365627-59-3
C₂₅H₃₂N₄O₄

Guidance literature:: With potassium tert-butylate; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1016/j.bmcl.2012.01.015

Reference yield:

: 1365627-76-4
C₁₅H₁₄ClN₃O

: 1365626-45-4
C₂₄H₂₉N₅OS

Guidance literature:: Multi-step reaction with 5 steps

1: potassium tert-butylate / acetonitrile / 2 h / 20 °C

2: dichloromethane / 2 h / 20 °C

3: sodium cyanoborohydride / 1,2-dichloro-ethane

4: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C

5: triethylsilane; trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

With triethylsilane; lithium aluminium tetrahydride; potassium tert-butylate; sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; acetonitrile;
DOI:10.1016/j.bmcl.2012.01.015