(+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate

Base Information

Chemical Name:(+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate
CAS No.:1256972-07-2
Molecular Formula:C₁₃H₂₁F₃O₂
Molecular Weight:266.304
Hs Code.:

Synonyms:(+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate

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Chemical Property of (+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate

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Technology Process of (+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate

There total 1 articles about (+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2516-99-6
3,3,3-Trifluoropropionic acid

: 2216-51-5
(-)-menthol

: 1256972-07-2
(+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/acs.joc.1c02288

Reference yield: 52.0%

: 123-75-1
pyrrolidine

: 1256972-07-2
(+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate

: (1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 5-(pyrrolidin-1-yl)-1H-1,2,3-triazole-4-carboxylate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; sodium azide; In tetrahydrofuran; at 50 ℃; for 12h; Schlenk technique;
DOI:10.1021/acs.joc.1c02288

Reference yield:

: 1256972-07-2
(+)-(1S,2R,5S)-2-isopropyl-5-methylcyclohexyl 3,3,3-trifluoropropanoate

: 100-52-7
benzaldehyde

: C₂₀H₂₇F₃O₃

: C₂₀H₂₇F₃O₃

Guidance literature:: With (-)-diisopinocampheylboron triflate; triethylamine; In dichloromethane; at -78 ℃; for 8h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.08.034