4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid

Base Information

Chemical Name:4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid
CAS No.:959992-08-6
Molecular Formula:C₁₈H₁₅Cl₂NO₅
Molecular Weight:396.227
Hs Code.:

Synonyms:4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid

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Chemical Property of 4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid

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Technology Process of 4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid

There total 2 articles about 4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 232276-45-8
N-(2,6-dichlorobenzoyl)-O-(trifluoromethanesulfonyl)-L-tyrosine methyl ester

: 141-53-7
sodium formate

: 959992-08-6
4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid

Guidance literature:: With acetic anhydride; lithium chloride; palladium diacetate; 1,3-bis-(diphenylphosphino)propane; In N,N-dimethyl-formamide; at 80 ℃; for 16h;

Reference yield:

: 959991-99-2
methyl (S)-2-(2,6-dichlorobenzamido)-3-(4-iodophenyl)propanoate

: 141-53-7
sodium formate

: 959992-08-6
4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid

Guidance literature:: methyl (S)-2-(2,6-dichlorobenzamido)-3-(4-iodophenyl)propanoate; sodium formate; With acetic anhydride; N-ethyl-N,N-diisopropylamine; lithium chloride; palladium 10% on activated carbon; In N,N-dimethyl-formamide; at 20 - 80 ℃;

With hydrogenchloride; In water; N,N-dimethyl-formamide;

Reference yield: 97.0%

: 959992-08-6
4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid

: methyl N-[(2,6-dichlorophenyl)carbonyl]-4-(hydroxymethyl)-L-phenylalaninate

Guidance literature:: 4-{(2S)-2-[(2,6-dichlorobenzoyl)amino]-3-methoxy-3-oxopropyl}benzoic acid; With borane dimethyl sulfide complex; In tetrahydrofuran; at 0 - 20 ℃; for 12h;

With methanol; In tetrahydrofuran;