N-amino(p-nitrophenyl)dichlorosulfurane

Base Information

• Chemical Name: N-amino(p-nitrophenyl)dichlorosulfurane
• CAS No.: 101414-51-1
• Molecular Formula: C₁₅H₁₄Cl₂N₂O₃S
• Molecular Weight: 373.26

Synonyms:N-amino(p-nitrophenyl)dichlorosulfurane

Chemical Property of N-amino(p-nitrophenyl)dichlorosulfurane

Chemical Property:

Purity/Quality:

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Technology Process of N-amino(p-nitrophenyl)dichlorosulfurane

There total 2 articles about N-amino(p-nitrophenyl)dichlorosulfurane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

ethyl N-(p-nitrophenylthio)benzenecarboximidate (101414-54-4) → N-amino(p-nitrophenyl)dichlorosulfurane (101414-51-1)

Guidance literature:

With chlorine; In diethyl ether; at 0 - 5 ℃;

Reference yield: 70.0%

4-nitrobenzenesulfenyl chloride (937-32-6) + N-chloro-benzimidic acid ethyl ester (33243-83-3) → N-amino(p-nitrophenyl)dichlorosulfurane (101414-51-1)

Guidance literature:

In diethyl ether; for 1h;

Reference yield: 100.0%

N-amino(p-nitrophenyl)dichlorosulfurane (101414-51-1) → ethyl N-(p-nitrophenylthio)benzenecarboximidate (101414-54-4)

Guidance literature:

With tris(dimethylamido)phosphite; In diethyl ether; at 0 ℃;

upstream raw materials:

4-nitrobenzenesulfenyl chloride

N-chloro-benzimidic acid ethyl ester

ethyl N-(p-nitrophenylthio)benzenecarboximidate

Downstream raw materials:

p-nitrobenzoyl-(N-benzoyl)-iminosulfinyl chloride

4-nitro-benzenesulfinyl chloride

ethyl benzimidate hydrochloride

p-nitrophenyl p-nitrobenzenethiosulfonate

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