(S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid

Base Information

Chemical Name:(S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid
CAS No.:117560-13-1
Molecular Formula:C₄H₄O₄*C₂₂H₃₅NO₄
Molecular Weight:493.598
Hs Code.:

Synonyms:(S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid

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Chemical Property of (S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid

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Technology Process of (S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid

There total 6 articles about (S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84277-81-6
L-2-aminodecanoic acid

: 117560-13-1
(S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: 36.7 percent / K₂CO₃ / dimethylsulfoxide / 30 h / Ambient temperature

3: ethyl acetate; diisopropyl ether

With thionyl chloride; potassium carbonate; In di-isopropyl ether; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm00122a003

Reference yield:

: 17702-88-4
rac-2-aminodecanoic acid

: 117560-13-1
(S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 92.1 percent

2: 47.5 percent / CoCl₂ / H₂O / 72 h / 37 °C / aminoacylase (from Aspergillus oryzae); pH 7

3: SOCl₂

4: 36.7 percent / K₂CO₃ / dimethylsulfoxide / 30 h / Ambient temperature

5: ethyl acetate; diisopropyl ether

With thionyl chloride; potassium carbonate; In di-isopropyl ether; water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm00122a003

Reference yield:

: 2623-95-2
2-bromodecanoic acid

: 117560-13-1
(S)-2-((S)-1-Benzyloxycarbonyl-ethylamino)-decanoic acid ethyl ester; compound with (Z)-but-2-enedioic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 62.9 percent / 28percent aq. NH₃ / 168 h / Ambient temperature

2: 92.1 percent

3: 47.5 percent / CoCl₂ / H₂O / 72 h / 37 °C / aminoacylase (from Aspergillus oryzae); pH 7

4: SOCl₂

5: 36.7 percent / K₂CO₃ / dimethylsulfoxide / 30 h / Ambient temperature

6: ethyl acetate; diisopropyl ether

With ammonium hydroxide; thionyl chloride; potassium carbonate; In di-isopropyl ether; water; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm00122a003