3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane

Base Information

Chemical Name:3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane
CAS No.:47702-79-4
Molecular Formula:C₃₀H₃₃NO
Molecular Weight:423.598
Hs Code.:

Synonyms:3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane

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Chemical Property of 3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane

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Technology Process of 3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane

There total 4 articles about 3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 47337-71-3
3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8-azabicyclo[3.2.1]octane

: 122-78-1
phenylacetaldehyde

: 47702-79-4
3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.12.008

Reference yield:

: 1210-33-9
5-chlorodibenzosuberane

: 47702-79-4
3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 20 °C

2: potassium permanganate; potassium hydroxide / pyridine; water / 5 h / 20 °C / Cooling with ice

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

With potassium permanganate; sodium tris(acetoxy)borohydride; potassium hydroxide; In pyridine; water; 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.bmcl.2011.12.008

Reference yield:

: 120-29-6
3-tropanol

: 47702-79-4
3α-((10,11-dihydro-5H-dibenzo[a,d]cyclohepten-5-yl)oxy)-8α-phenetyl-8-azabicyclo[3.2.1]octane

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 20 °C

2: potassium permanganate; potassium hydroxide / pyridine; water / 5 h / 20 °C / Cooling with ice

3: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C / Inert atmosphere

With potassium permanganate; sodium tris(acetoxy)borohydride; potassium hydroxide; In pyridine; water; 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.bmcl.2011.12.008