1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine

Base Information

Chemical Name:1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine
CAS No.:1374877-03-8
Molecular Formula:C₄₆H₈₄N₂O₄S₃
Molecular Weight:825.382
Hs Code.:

Synonyms:1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine

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Chemical Property of 1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine

Chemical Property:

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Technology Process of 1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine

There total 3 articles about 1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 870-50-8
di-tert-butyl-diazodicarboxylate

: 1372535-59-5
1-bromo-3,4,5-tridecylsulfanylbenzene

: 1374877-03-8
1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine

Guidance literature:: 1-bromo-3,4,5-tridecylsulfanylbenzene; With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 1.5h; Inert atmosphere;

di-tert-butyl-diazodicarboxylate; In tetrahydrofuran; pentane; at -78 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.3762/bjoc.8.29

Reference yield:

: 40520-16-9
sodium n-decylthiolate

: 1374877-03-8
1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 - 80 °C

2: tert.-butyl lithium / tetrahydrofuran

With tert.-butyl lithium; In tetrahydrofuran;
DOI:10.1080/10426507.2012.736896

Reference yield:

: 138526-69-9
3,4,5-trifluoro-1-bromobenzene

: 1374877-03-8
1,2-bis(tert-butoxycarbonyl)-1-(3,4,5-tridecylsulfanylphenyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 60 - 80 °C

2: tert.-butyl lithium / tetrahydrofuran

With tert.-butyl lithium; In tetrahydrofuran;
DOI:10.1080/10426507.2012.736896