1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete

Base Information

Chemical Name:1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete
CAS No.:504435-31-8
Molecular Formula:C₃₁H₅₉N₄PSi
Molecular Weight:546.896
Hs Code.:

Synonyms:1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete

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Chemical Property of 1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete

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Technology Process of 1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete

There total 2 articles about 1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1467-79-4
NCNMe₂

: 152387-46-7,156280-08-9
[bis(dicyclohexylamino)phosphino](trimethylsilyl)carbene

: 504435-31-8
1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete

Guidance literature:: In toluene; at 20 ℃;
DOI:10.1002/1521-3765(20021202)8:23<5305::AID-CHEM5305>3.0.CO;2-6

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 504435-32-9
C₂₈H₅₁N₄P

: 504435-31-8
1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete

Guidance literature:: C₂₈H₅₁N₄P; With lithium diisopropyl amide; In tetrahydrofuran; at 0 ℃; for 0.75h;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 - 0 ℃; for 0.5h; Further stages.;
DOI:10.1002/1521-3765(20021202)8:23<5305::AID-CHEM5305>3.0.CO;2-6

Reference yield:

: 504435-31-8
1,3-bis(dicyclohexylamino)-4-dimethylamino-2-trimethylsilyl-1,2-dihydro-1,2-azaphosphete

: 504435-32-9
C₂₈H₅₁N₄P

Guidance literature:: With tetrabutyl ammonium fluoride; In toluene; at 20 ℃; for 1h;
DOI:10.1002/1521-3765(20021202)8:23<5305::AID-CHEM5305>3.0.CO;2-6