1-Dimethoxymethyl-4-iodo-benzene

Base Information

Chemical Name:1-Dimethoxymethyl-4-iodo-benzene
CAS No.:99405-03-5
Molecular Formula:C9H11 I O2
Molecular Weight:278.09
Hs Code.:2909309090
European Community (EC) Number:619-431-6
DSSTox Substance ID:DTXSID40465194
Nikkaji Number:J3.189.509J
Wikidata:Q82290965
Mol file:99405-03-5.mol

Synonyms:99405-03-5;4-IODOBENZALDEHYDE DIMETHYL ACETAL;1-dimethoxymethyl-4-iodo-benzene;p-iodobenzaldehyde dimethyl acetal;SCHEMBL347953;DTXSID40465194;AFFDFWRTCGIWLL-UHFFFAOYSA-N;1-Iodo-4-(1,1-dimethoxymethyl)benzene

Suppliers and Price of 1-Dimethoxymethyl-4-iodo-benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Dimethoxymethyl-4-iodo-benzene

Chemical Property:

PSA：18.46000
LogP:2.58260
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:277.98038
Heavy Atom Count:12
Complexity:118

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(C1=CC=C(C=C1)I)OC

Technology Process of 1-Dimethoxymethyl-4-iodo-benzene

There total 2 articles about 1-Dimethoxymethyl-4-iodo-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 149-73-5
trimethyl orthoformate

: 99405-03-5
1-iodo-4-(1,1-dimethoxymethyl)benzene

Guidance literature:: p-(iodophenyl)carboxaldehyde; trimethyl orthoformate; With toluene-4-sulfonic acid; In methanol; at 20 ℃; for 3h;

With sodium hydrogencarbonate; In methanol; for 1h;

Reference yield: 96.0%

: 67-56-1
methanol

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 99405-03-5
1-iodo-4-(1,1-dimethoxymethyl)benzene

Guidance literature:: With TEA; titanium tetrachloride; at 20 ℃; for 0.25h;
DOI:10.1021/jo049439q

Reference yield: 91.0%

: 99405-03-5
1-iodo-4-(1,1-dimethoxymethyl)benzene

: 1066-54-2
trimethylsilylacetylene

: 193212-16-7
((4-(dimethoxymethyl)phenyl)ethynyl)trimethylsilane

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-butylamine; In toluene; for 28h; Ambient temperature;
DOI:10.1039/a700234c