(E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

Base Information

Chemical Name:(E)-1-phenylethan-1-one O-perfluorobenzoyl oxime
CAS No.:479675-59-7
Molecular Formula:C₁₅H₈F₅NO₂
Molecular Weight:329.226
Hs Code.:

Synonyms:(E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

Suppliers and Price of (E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

There total 3 articles about (E)-1-phenylethan-1-one O-perfluorobenzoyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 10341-75-0
(E)-1-phenylethanone oxime

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: 479675-59-7
(E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1021/ol070561w

Reference yield:

: 613-91-2
acetophenone oxime

pentafluorobenzoylchloride: 2251-50-5
pentafluorobenzoylchloride

: 479675-59-7
(E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; Cooling with ice;
DOI:10.1002/anie.200804683

Reference yield:

: 98-86-2
acetophenone

: 479675-59-7
(E)-1-phenylethan-1-one O-perfluorobenzoyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol / Inert atmosphere; Sealed tube

2: pyridine / dichloromethane / 0 °C / Inert atmosphere; Sealed tube

With pyridine; hydroxylamine hydrochloride; sodium acetate; In ethanol; dichloromethane;
DOI:10.1002/anie.202006740