1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene

Base Information

• Chemical Name: 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene
• CAS No.: 89738-82-9
• Molecular Formula: C₂₇H₄₈S
• Molecular Weight: 404.744

Synonyms:1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene

Chemical Property of 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene

There total 8 articles about 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

t-butyl-2,2-dimethyl-1-(1,3,5-tri-t-butylbicyclo<2.2.0>hexa-2,5-dien-2-yl)propyl sulfide (92635-34-2) → 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene (89738-82-9)

Guidance literature:

In benzene; at 200 ℃; for 4h;

DOI:10.1016/S0040-4039(01)80044-7

Reference yield: 31.0%

tert-butylmagnesium chloride (677-22-5) + 2,4,6-tri-(tert-butyl)thiobenzaldehyde (84543-57-7) → 3,5-tri-t-butyl-2-(t-butylthiomethyl)benzene (89738-81-8) + 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene (89738-82-9) + 1,2-Bis-(2,4,6-tri-tert-butyl-phenyl)-ethane-1,2-dithiol (89738-83-0)

Guidance literature:

In diethyl ether; at 0 ℃; Product distribution; Mechanism; first example of dimerization of thioketyl radicals;

DOI:10.1246/cl.1984.101

Reference yield: 23.0%

tert.-butyl lithium (594-19-4) + 2,4,6-tri-(tert-butyl)thiobenzaldehyde (84543-57-7) → 3,5-tri-t-butyl-2-(t-butylthiomethyl)benzene (89738-81-8) + 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene (89738-82-9) + 2,2-Dimethyl-1-(2,4,6-tri-tert-butyl-phenyl)-propane-1-thiol + 1,2-Bis-(2,4,6-tri-tert-butyl-phenyl)-ethane-1,2-dithiol (89738-83-0)

Guidance literature:

Further byproducts given;

upstream raw materials:

tert.-butyl lithium

2,4,6-tri-(tert-butyl)thiobenzaldehyde

tert-butylmagnesium chloride

t-butyl-2,2-dimethyl-1-(1,3,5-tri-t-butylbicyclo<2.2.0>hexa-2,5-dien-2-yl)propyl sulfide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 89738-82-9 1,3,5-Tri-tert-butyl-2-(1-tert-butylsulfanyl-2,2-dimethyl-propyl)-benzene

Send

Send

Metric Ton KG G Pound L ML

Send

Send