benzyl 5-methyl-3-oxa-5-hexenoate

Base Information

Chemical Name:benzyl 5-methyl-3-oxa-5-hexenoate
CAS No.:914092-04-9
Molecular Formula:C₁₃H₁₆O₃
Molecular Weight:220.268
Hs Code.:

Synonyms:benzyl 5-methyl-3-oxa-5-hexenoate

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Chemical Property of benzyl 5-methyl-3-oxa-5-hexenoate

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Technology Process of benzyl 5-methyl-3-oxa-5-hexenoate

There total 1 articles about benzyl 5-methyl-3-oxa-5-hexenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 10041-27-7
[(2-methylprop-2-en-1-yl)oxy]acetic acid

: 100-51-6,185532-71-2
benzyl alcohol

: 914092-04-9
benzyl 5-methyl-3-oxa-5-hexenoate

Guidance literature:: With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1246/bcsj.79.1275

Reference yield:

: 914092-04-9
benzyl 5-methyl-3-oxa-5-hexenoate

: benzyl 2-hydroxy-4-methyl-4-pentenoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 76 percent Spectr_. / lithium hexamethyldisilazide / tetrahydrofuran; hexane / -78 - 20 °C

2.1: tetrabutylammonium 4-methoxybenzoate / dimethylformamide / 3 h / 20 °C

2.2: 40 percent / HCl / dimethylformamide; H₂O / 0.5 h

With 4-methoxybenzoate, tetrabutylammonium salt; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; N,N-dimethyl-formamide; 2.1: <2,3>-Wittig rearrangement;
DOI:10.1246/bcsj.79.1275

Reference yield:

: 914092-04-9
benzyl 5-methyl-3-oxa-5-hexenoate

: 75-77-4
chloro-trimethyl-silane

: 1-benzyloxy-5-methyl-1-trimethylsilyloxy-3-oxa-1,5-hexadiene

Guidance literature:: benzyl 5-methyl-3-oxa-5-hexenoate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃;

chloro-trimethyl-silane; In tetrahydrofuran; at -78 ℃;
DOI:10.1246/cl.2005.1188