(S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate
CAS No.:210533-63-4
Molecular Formula:C₁₇H₂₆N₂O₄
Molecular Weight:322.404
Hs Code.:

Synonyms:(S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate

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Chemical Property of (S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate

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Technology Process of (S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate

There total 4 articles about (S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 60398-41-6
(3S)-tert-butyl 1-benzyl-3-diazo-2-oxopropylcarbamate

: 1117-97-1
N,0-dimethylhydroxylamine

: 210533-63-4
(S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate

Guidance literature:: With silver benzoate; triethylamine; In tetrahydrofuran; at -25 ℃; for 2h;
DOI:10.1016/S0040-4039(98)00675-3

Reference yield:

: 51871-62-6
(S)-3-tert-butoxycarbonylamino-4-phenylbutanoic acid

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 210533-63-4
(S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate

Guidance literature:: With benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1016/S0960-894X(02)00840-5

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 210533-63-4
(S)-tert-butyl 4-(methoxy(methyl)amino)-4-oxo-1-phenylbutan-2-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: NMM / tetrahydrofuran / 1 h / -25 °C

2: diethyl ether / 2 h / Ambient temperature

3: 94 percent / Et₃N, C₆H₅CO₂Ag / tetrahydrofuran / 2 h / -25 °C

With 4-methyl-morpholine; silver benzoate; triethylamine; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4039(98)00675-3