1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane

Base Information

• Chemical Name: 1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane
• CAS No.: 172607-40-8
• Molecular Formula: C₁₃H₁₆O₄
• Molecular Weight: 236.268
• Mol file: 172607-40-8.mol

Synonyms:1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane

Chemical Property of 1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane

There total 1 articles about 1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.5%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + acetophenone (98-86-2) → 1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane (172607-40-8)

Guidance literature:

With calcium oxide; In water; at 60 ℃; for 5h;

Reference yield: 50.0%

1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane (172607-40-8) → (3-bromo-2-(bromomethyl)prop-1-en-1-yl)benzene (161152-94-9)

Guidance literature:

With hydrogen bromide; In water; Heating;

DOI:10.1080/00397919908085884

Reference yield: 48.0%

1-phenyl-2,4,8,10 tetra oxaspiro<5.5> undecane (172607-40-8) → α,α'-bis(methylene chloride) β-phenyl ethene (172607-41-9)

Guidance literature:

With hydrogenchloride; zinc(II) chloride; Heating;

DOI:10.1080/00397919508011456

upstream raw materials:

formaldehyd

acetophenone

Downstream raw materials:

α,α'-bis(methylene chloride) β-phenyl ethene

(3-bromo-2-(bromomethyl)prop-1-en-1-yl)benzene

C₁₁H₁₃Br₃O