4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

Base Information

Chemical Name:4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane
CAS No.:247153-37-3
Molecular Formula:C₂₆H₃₈N₂O₆S
Molecular Weight:506.664
Hs Code.:

Synonyms:4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

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Chemical Property of 4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

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Technology Process of 4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

There total 4 articles about 4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 100-46-9
benzylamine

: 9-[(4-methylphenyl)sulfonyl]-3,6,12,15-tetraoxa-9-aza-1,17-heptadecanediyl bis(methanesulfonate)

: 247153-37-3
4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

Guidance literature:: With sodium carbonate; In acetonitrile; for 72h; Heating;
DOI:10.1016/S0040-4020(99)00573-6

Reference yield:

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 247153-37-3
4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 87.5 percent / K₂CO₃ / dimethylformamide / 96 h / 100 °C

2: 98.4 percent / pyridine

3: 45 percent / Na₂CO₃ / acetonitrile / 72 h / Heating

With pyridine; sodium carbonate; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; 1: Alkylation / 2: Esterification / 3: Cyclization;
DOI:10.1016/S0040-4020(99)00573-6

Reference yield:

: 70-55-3
toluene-4-sulfonamide

: 247153-37-3
4-benzyl-13-[(4-methylphenyl)sulfonyl]-1,7,10,16-tetraoxa-4,13-diazacyclooctadecane

Guidance literature:: Multi-step reaction with 3 steps

1: 87.5 percent / K₂CO₃ / dimethylformamide / 96 h / 100 °C

2: 98.4 percent / pyridine

3: 45 percent / Na₂CO₃ / acetonitrile / 72 h / Heating

With pyridine; sodium carbonate; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; 1: Alkylation / 2: Esterification / 3: Cyclization;
DOI:10.1016/S0040-4020(99)00573-6