C₃₀H₃₉BrN₂O₆S

Base Information

Chemical Name:C₃₀H₃₉BrN₂O₆S
CAS No.:1434649-75-8
Molecular Formula:C₃₀H₃₉BrN₂O₆S
Molecular Weight:635.619
Hs Code.:

C<sub>30</sub>H<sub>39</sub>BrN<sub>2</sub>O<sub>6</sub>S

Synonyms:C₃₀H₃₉BrN₂O₆S

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Chemical Property of C₃₀H₃₉BrN₂O₆S

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Technology Process of C₃₀H₃₉BrN₂O₆S

There total 9 articles about C₃₀H₃₉BrN₂O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 1434644-94-6
C₂₉H₃₅BrN₂O₆S

: 676-58-4
methylmagnesium chloride

: 1434649-75-8
C₃₀H₃₉BrN₂O₆S

Guidance literature:: With ammonium chloride; In tetrahydrofuran; at -78 - -50 ℃; for 4h; Inert atmosphere;

Reference yield:

: 4815-30-9
diethyl 5-amino-3-methyl-2,4-thiophenedicarboxylate

: 1434649-75-8
C₃₀H₃₉BrN₂O₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C

1.2: 10 - 100 °C

2.1: sodium hydroxide; water / methanol / 4 h / 50 °C

3.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C

4.1: bromine; CH₃COONa / acetic acid / 1 h / 20 °C

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

6.1: ammonium chloride / tetrahydrofuran / 4 h / -78 - -50 °C / Inert atmosphere

With 1-methyl-pyrrolidin-2-one; di-isopropyl azodicarboxylate; CH₃COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; ammonium chloride; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; acetic acid;

Reference yield:

: 4512-32-7
H-Aib-OtBu

: 1434649-75-8
C₃₀H₃₉BrN₂O₆S

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 5.5 h / 0 - 20 °C

2.1: sodium hydride / 1,4-dioxane / 0.25 h / 10 °C

2.2: 10 - 100 °C

3.1: sodium hydroxide; water / methanol / 4 h / 50 °C

4.1: potassium carbonate; silver(I) acetate; 1-methyl-pyrrolidin-2-one / 2 h / 110 °C

5.1: bromine; CH₃COONa / acetic acid / 1 h / 20 °C

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

7.1: ammonium chloride / tetrahydrofuran / 4 h / -78 - -50 °C / Inert atmosphere

With 1-methyl-pyrrolidin-2-one; di-isopropyl azodicarboxylate; CH₃COONa; water; bromine; silver(I) acetate; sodium hydride; potassium carbonate; ammonium chloride; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; acetic acid;