(2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester

Base Information

Chemical Name:(2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester
CAS No.:850404-73-8
Molecular Formula:C₂₂H₃₅NO₈
Molecular Weight:441.522
Hs Code.:

Synonyms:(2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester

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Chemical Property of (2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester

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Technology Process of (2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester

There total 1 articles about (2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (E)-3-(3,5-Diisopropoxy-4-methoxy-phenyl)-acrylic acid methyl ester

: 4248-19-5
tert-butyl carbazate

: (2S,3R)-2-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-3-hydroxy-propionic acid methyl ester

: 850404-73-8
(2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester

: 2,2-bis-tert-butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-3-oxo-propionic acid methyl ester

: 171738-31-1
4-methoxy-3,5-diisopropyloxybenzaldehyde

Guidance literature:: With sodium hydroxide; tert-butylhypochlorite; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium dioxotetrahydroxoosmate(VI); In propan-1-ol; water; at 10 ℃; for 1h;
DOI:10.1021/jo047772o

Reference yield: 98.0%

: 850404-73-8
(2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester

: 124-63-0
methanesulfonyl chloride

: 850404-77-2
(2S,3R)-3-tert-butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxyphenyl)-2-methanesulfonyloxypropionic acid methyl ester

Guidance literature:: With pyridine; at 0 - 20 ℃; for 4h;
DOI:10.1021/jo047772o

Reference yield:

: 850404-73-8
(2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid methyl ester

: 71-23-8
propan-1-ol

: 4-methoxy-3,5-diisopropyloxybenzoic acid

: (2S,3R)-3-tert-Butoxycarbonylamino-3-(3,5-diisopropoxy-4-methoxy-phenyl)-2-hydroxy-propionic acid propyl ester

Guidance literature:: With sodium hydroxide; potassium dioxotetrahydroxoosmate(VI); 1,4-bis(9-O-dihydroquinidine)phthalazine; tert-butyl carbazate; In water; for 3h;
DOI:10.1021/jo047772o