1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride

Base Information

• Chemical Name: 1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride
• CAS No.: 1404118-95-1
• Molecular Formula: C₂₄H₃₁N₄*Cl
• Molecular Weight: 410.99
• Mol file: 1404118-95-1.mol

Synonyms:1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride

Chemical Property of 1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride

There total 1 articles about 1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

N-(2,6-dimethylphenyl)acetimidoyl chloride2 (157894-09-2) + 1-(1-(2,6-dimethylphenylimino)ethyl)-4,5,6-trihydropyrimidine → 1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride (1404118-95-1)

Guidance literature:

In benzene; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.1021/om300873k

Reference yield: 76.0%

copper(l) iodide (7681-65-4) + 1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride (1404118-95-1) → [1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidin-2-ylidene]copper(I) iodide

Guidance literature:

copper(l) iodide; With sodium hexamethyldisilazane; In tetrahydrofuran; at -37 ℃; Inert atmosphere;

1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride; In tetrahydrofuran; at -37 - 20 ℃; Inert atmosphere;

DOI:10.1021/om300873k

Reference yield:

C6H18NSi2(1-)*Fe(2+)*Cl(1-) + 1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidinium chloride (1404118-95-1) → [1,3-bis[1-(2,6-dimethylphenylimino)ethyl]-4,5,6-trihydropyrimidin-2-ylidene]iron(II) dihloride

Guidance literature:

In tetrahydrofuran; at -37 - 20 ℃; Inert atmosphere;

DOI:10.1021/om300873k

upstream raw materials:

N-(2,6-dimethylphenyl)acetimidoyl chloride2