Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

Base Information

Chemical Name:Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile
CAS No.:121056-90-4
Molecular Formula:C₂₉H₅₇NO₃Si₄
Molecular Weight:580.118
Hs Code.:

Synonyms:Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

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Chemical Property of Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

Chemical Property:

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Technology Process of Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

There total 5 articles about Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99-24-1
methyl galloate

: 121056-90-4
Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / imidazole / dimethylformamide / 20 h

2: 79 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / Ambient temperature

4: ZnI₂ / 4 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; pyridinium chlorochromate; zinc(II) iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00198a040

Reference yield:

: 121056-97-1
methyl 3,4,5-tris<(tert-butyldimethylsilyl)oxy>benzoate

: 121056-90-4
Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

2: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / Ambient temperature

3: ZnI₂ / 4 h / Ambient temperature

With lithium aluminium tetrahydride; pyridinium chlorochromate; zinc(II) iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja00198a040

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 121056-90-4
Trimethylsilanyl-[3,4,5-tris-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acetonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / imidazole / dimethylformamide / 20 h

2: 79 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 75 percent / pyridinium chlorochromate / CH₂Cl₂ / 4 h / Ambient temperature

4: ZnI₂ / 4 h / Ambient temperature

With 1H-imidazole; lithium aluminium tetrahydride; pyridinium chlorochromate; zinc(II) iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00198a040