Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz

Base Information

• Chemical Name: Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz
• CAS No.: 79227-87-5
• Molecular Formula: C₆H₆ClO₄P*C₆H₁₃N
• Molecular Weight: 307.714
• Mol file: 79227-87-5.mol

Synonyms:Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz

Chemical Property of Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz

Chemical Property:

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Technology Process of Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz

There total 2 articles about Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.5%

tris(p-chlorophenyl)phosphite (5679-61-8) + cyclohexylamine (108-91-8,157973-60-9) → 4-chlorophenyl phosphate (13388-88-0) + Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz (79227-87-5)

Guidance literature:

With phosphoric acid; In nitromethane; at 100 ℃; for 5h;

Reference yield:

→ Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz (79227-87-5)

Guidance literature:

entspr. Phosphoroxydichlorid 1. H2O 2. /BRN= 471175/;

DOI:10.1016/0040-4020(75)80096-2

Reference yield: 82.5%

triphenyl phosphite (101-02-0) + Phosphorsaeure-p-chlorphenylester Cyclohexylammonium salz (79227-87-5) + cyclohexylamine (108-91-8,157973-60-9) → Phosphorsaeure-p-chlorphenylester-phenylester (59447-19-7) + Phosphorsaeure-p-chlorphenylester-phenylester Cyclohexylammonium salz (59447-20-0)

Guidance literature:

In nitromethane; at 100 ℃; for 5h;

upstream raw materials:

tris(p-chlorophenyl)phosphite

cyclohexylamine

Downstream raw materials:

Phosphorsaeure-p-chlorphenylester-phenylester

Phosphorsaeure-p-chlorphenylester-phenylester Cyclohexylammonium salz