CARBAZOLE (RING-D8)

Base Information

• Chemical Name: CARBAZOLE (RING-D8)
• CAS No.: 97960-57-1
• Molecular Formula: C₁₂H₉N
• Molecular Weight: 167.21
• Mol file: 97960-57-1.mol

Synonyms:CARBAZOLE (RING-D8);CARBAZOLE-D8, NH;CARBAZOLE-D8

Chemical Property of CARBAZOLE (RING-D8)

Chemical Property:

• PSA: 15.79000
• LogP: 3.32110

Purity/Quality:

99% ^*data from raw suppliers

CARBAZOLE(RING-D8) 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CARBAZOLE (RING-D8)

There total 581 articles about CARBAZOLE (RING-D8) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

9-(1-methoxy-2-propynyl)carbazole → Propargylic aldehyde (624-67-9) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1)

Guidance literature:

With sulfuric acid; In 1,4-dioxane; at 18 ℃;

DOI:10.1023/A:1012341921034

Reference yield: 81.0%

2-(diphenylamino)isoindoline-1,3-dione (6295-93-8) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 4-phenyldiphenylamine (32228-99-2) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1)

Guidance literature:

With aluminium trichloride; at 20 ℃; for 4h;

DOI:10.1021/jo016124r

Reference yield: 78.0%

9-(4-Benzyloxy-benzyl)-9H-carbazole (205578-45-6) → p-benzyloxybenzaldehyde (4397-53-9) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; at 80 ℃; for 101h;

DOI:10.3987/COM-97-7990

upstream raw materials:

brucine

tetrachloromethane

2,3,4,5,6,7,8,9-octahydro-1H-carbazole

chloranil

Downstream raw materials:

9-(2-pyridyl)carbazole

N-<(phenylthio)methyl>carbazole

1,3,6,8-tetra-tert-butyl-9H-carbazole

1-Carbazol-9-yl-2-o-tolyloxy-ethanone

Refernces

• 1、 Manna, Kartic,Ganguly, Tanusree,Baitalik, Sujoy,Jana, Ranjan. "Visible-Light- And PPh3-Mediated Direct C-N Coupling of Nitroarenes and Boronic Acids at Ambient Temperature". supporting information. p. 8634 - 8639. Retrieved 2021/11/01.
• 2、 -. "Preparation method of 3 - bromo - N - phenyl carbazole". . . Retrieved 2021/10/11.