(S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol

Base Information

Chemical Name:(S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol
CAS No.:957782-23-9
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:(S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol

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Technology Process of (S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol

There total 3 articles about (S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₄O₅

: 957782-23-9
(S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol

Guidance literature:: With methanol; potassium hydroxide; In dichloromethane; at 20 ℃;
DOI:10.1021/jo701524p

Reference yield:

: 663942-91-4
(2S,3R,4R)-3,5-dihydroxy-2,4-dimethylpentyl acetate

: 957782-23-9
(S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: p-toluenesulfonic acid monohydrate / CH₂Cl₂ / 4 h

2: 72.0 mg / KOH; MeOH / CH₂Cl₂ / 20 °C

With methanol; potassium hydroxide; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1021/jo701524p

Reference yield:

: 171019-25-3
acetic acid (2S,3R,4R)-3-(tert-butyldimethylsilanyloxy)-5-hydroxy-2,4-dimethylpentyl ester

: 957782-23-9
(S)-2-((2R,4S,5R)-2-(4-methoxyphenyl)-5-methyl-1,3-dioxan-4-yl)propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / glacial acetic acid; tetrabutylammonium fluoride / tetrahydrofuran / 12 h / 20 °C

2: p-toluenesulfonic acid monohydrate / CH₂Cl₂ / 4 h

3: 72.0 mg / KOH; MeOH / CH₂Cl₂ / 20 °C

With methanol; potassium hydroxide; tetrabutyl ammonium fluoride; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo701524p