methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate

Base Information

Chemical Name:methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate
CAS No.:1286280-77-0
Molecular Formula:C₁₉H₂₉NO₅
Molecular Weight:351.443
Hs Code.:

Synonyms:methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate

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Chemical Property of methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate

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Technology Process of methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate

There total 2 articles about methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1286280-77-0
methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

With di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 57591-61-4,68697-60-9,127369-30-6,134694-94-3
methyl (R)-2-amino-2-(4-hydroxyphenyl)acetate hydrochloride

: 1286280-77-0
methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

With di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;

Reference yield: 88.0%

: 1286280-77-0
methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate

: 1286280-51-0
{(R)-2-hydroxy-1-[4-((S)-2-methyl-butoxy)phenyl]ethyl}carbamic acid t-butyl ester

Guidance literature:: methyl (2R)-2-{[(tert-butoxy)carbonyl]amino}-2-{4-[(2S)-2-methylbutoxy]phenyl}acetate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

With potassium hydroxide; In tetrahydrofuran; water; ethyl acetate; for 1h;