N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

Base Information

Chemical Name:N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine
CAS No.:927652-16-2
Molecular Formula:C₂₉H₄₅N₃O₆Si₂
Molecular Weight:587.864
Hs Code.:

N<sup>4</sup>-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

Synonyms:N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

Suppliers and Price of N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

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Technology Process of N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

There total 4 articles about N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-31-3
Methyl formate

: 51549-38-3
N⁴-benzoyl-O^3',O^5'-bis(tert-butyldimethylsilyl)-2'-deoxycytidine

: 927652-16-2
N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

Guidance literature:: N⁴-benzoyl-O^3',O^5'-bis(tert-butyldimethylsilyl)-2'-deoxycytidine; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 4h;

Methyl formate; In tetrahydrofuran; at -78 ℃; for 3h; Further stages.;
DOI:10.3987/com-06-s(o)3

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 927652-16-2
N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: imidazole / dimethylformamide / 4 h / 20 °C

1.2: 99 percent / dimethylformamide / 0.25 h / 160 °C / microwave irradiation

2.1: LDA / tetrahydrofuran / 4 h / -78 °C

2.2: tetrahydrofuran / 3 h / -78 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.3987/com-06-s(o)3

Reference yield:

: 93-97-0
benzoic acid anhydride

: 927652-16-2
N⁴-benzoyl-3',5'-bis-O-(tert-butyldimethylsilyl)-6-formyl-2'-deoxycytidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: imidazole / dimethylformamide / 4 h / 20 °C

1.2: 99 percent / dimethylformamide / 0.25 h / 160 °C / microwave irradiation

2.1: LDA / tetrahydrofuran / 4 h / -78 °C

2.2: tetrahydrofuran / 3 h / -78 °C

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.3987/com-06-s(o)3