2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene

Base Information

Chemical Name:2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene
CAS No.:862731-94-0
Molecular Formula:C₁₅H₉F₆O₃P
Molecular Weight:382.199
Hs Code.:

Synonyms:2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene

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Technology Process of 2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene

There total 1 articles about 2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1641-40-3
pyrocatechol phosphorochloridite

: 721-36-8
α-trifluoromethyl-m-trifluoromethylbenzyl alcohol

: 862731-94-0
2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene

Guidance literature:: With pyridine; In diethyl ether; hexane; at 20 ℃;
DOI:10.1016/j.jorganchem.2005.04.038

Reference yield: 53.0%

: 862731-94-0
2-[2,2,2-trifluoro-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene

: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer

: 75-09-2
dichloromethane

: 862732-01-2
[(η5-pentamethylcyclopentadienyl)RhCl2(2-[2,2,2-trifluo-1-[3-(trifluoromethyl)phenyl]ethoxy]-1,3,2-benzodioxaphospholene)]

Guidance literature:: In dichloromethane; under inert atm. of dry Ar using Schlenk and vac. line techniques; to soln. of Rh complex in CH2Cl2 added soln. of ligand in CH2Cl2; mixt. stirred for 1 h at room temp.; solvent evapd. (vac.); pentane added; crystals filtered off; dried (vac.); elem. anal.;
DOI:10.1016/j.jorganchem.2005.04.038