methyl Z-4-methylstyrylsulfoyl acetate

Base Information

• Chemical Name: methyl Z-4-methylstyrylsulfoyl acetate
• CAS No.: 170884-91-0
• Molecular Formula: C₁₂H₁₄O₄S
• Molecular Weight: 254.307
• Mol file: 170884-91-0.mol

Synonyms:methyl Z-4-methylstyrylsulfoyl acetate

Chemical Property of methyl Z-4-methylstyrylsulfoyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of methyl Z-4-methylstyrylsulfoyl acetate

There total 3 articles about methyl Z-4-methylstyrylsulfoyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

methanol (67-56-1) + Z-4-methylstyrylsulfonyl acetic acid (155782-80-2) → methyl Z-4-methylstyrylsulfoyl acetate (170884-91-0)

Guidance literature:

With sulfuric acid; for 5h; Heating;

Reference yield:

4-n-methylphenylacetylene (766-97-2) → methyl Z-4-methylstyrylsulfoyl acetate (170884-91-0)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOH / methanol

2: 30percent H₂O₂, gl. AcOH

3: 70 percent / conc. H₂SO₄ / 5 h / Heating

With sodium hydroxide; sulfuric acid; dihydrogen peroxide; acetic acid; In methanol;

Reference yield:

Z-4-methylstyrylthioacetic acid (155782-81-3) → methyl Z-4-methylstyrylsulfoyl acetate (170884-91-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 30percent H₂O₂, gl. AcOH

2: 70 percent / conc. H₂SO₄ / 5 h / Heating

With sulfuric acid; dihydrogen peroxide; acetic acid;

upstream raw materials:

methanol

Z-4-methylstyrylsulfonyl acetic acid

Z-4-methylstyrylthioacetic acid

4-n-methylphenylacetylene