1-(3-METHOXY-PHENYL)-2-METHYLAMINO-ETHANOL

Base Information

• Chemical Name: 1-(3-METHOXY-PHENYL)-2-METHYLAMINO-ETHANOL
• CAS No.: 92188-49-3
• Molecular Formula: C10H15NO2
• Molecular Weight: 181.235
• Hs Code.: 2922509090
• Mol file: 92188-49-3.mol

Synonyms:Benzylalcohol, m-methoxy-a-[(methylamino)methyl]- (6CI,7CI);(?à)-2-Methylamino-1-(3-methoxyphenyl)ethanol;1-(3-Methoxyphenyl)-2-(methylamino)ethanol;

Chemical Property of 1-(3-METHOXY-PHENYL)-2-METHYLAMINO-ETHANOL

Chemical Property:

• Vapor Pressure: 0.000185mmHg at 25°C
• Refractive Index: 1.527
• Boiling Point: 315.4 °C at 760 mmHg
• Flash Point: 144.6 °C
• PSA: 41.49000
• Density: 1.067 g/cm³
• LogP: 1.33890

Purity/Quality:

97% ^*data from raw suppliers

1-(3-Methoxyphenyl)-2-(methylamino)ethanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(3-METHOXY-PHENYL)-2-METHYLAMINO-ETHANOL

There total 5 articles about 1-(3-METHOXY-PHENYL)-2-METHYLAMINO-ETHANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(m-methoxyphenyl)oxirane (32017-77-9,53631-49-5) + methylamine (74-89-5) → 1-(3-methoxyphenyl)-2-methylaminoethanol (92188-49-3)

Guidance literature:

In methanol; at 60 - 100 ℃;

DOI:10.1016/j.bmcl.2007.03.102

Reference yield:

Phenylephrine (1477-63-0) → 1-(3-methoxyphenyl)-2-methylaminoethanol (92188-49-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 62.5 percent / sodium acetate / H₂O / 4 h / 20 °C

2: sodium ethylate / ethanol / 2 h / Heating

With sodium ethanolate; sodium acetate; In ethanol; water;

DOI:10.1007/BF00772946

Reference yield:

N-acetyl-1-(3-hydroxyphenyl)-2-methylaminoethanol (69728-91-2) + methyl iodide (74-88-4) → 1-(3-methoxyphenyl)-2-methylaminoethanol (92188-49-3)

Guidance literature:

With sodium ethanolate; In ethanol; for 2h; Yield given; Heating;

DOI:10.1007/BF00772946

upstream raw materials:

N-acetyl-1-(3-hydroxyphenyl)-2-methylaminoethanol

methyl iodide

2-(m-methoxyphenyl)oxirane

methylamine

Downstream raw materials:

C₂₇H₂₈N₃SO₄Cl

2-methylamino-N-nitroso-1-(m-methoxyphenyl)-1-ethanol

rac N-(4-chlorobenzyl)-9-{[[2-hydroxy-2-(3-methoxyphenyl)ethyl](methyl)amino]methyl}-1-methyl-2,7-dioxo-2,3-dihydro-1H,7H-pyrido[1,2,3-de]quinoxaline-6-carboxamide

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