1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid

Base Information

Chemical Name:1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid
CAS No.:97095-06-2
Molecular Formula:C₂₇H₂₅NO₄
Molecular Weight:427.5
Hs Code.:

1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzo<c>phenanthren-4a-carboxamid

Synonyms:1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid

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Chemical Property of 1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid

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Technology Process of 1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid

There total 4 articles about 1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 64678-90-6
N-(4-Methoxyphenyl)-3-oxo-3H-naphtho<2,1-b>pyran-2-carboxamid

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 97095-06-2
1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid

Guidance literature:: With hydroquinone; In toluene; at 110 - 120 ℃; for 168h;
DOI:10.1002/jlac.198519850504

Reference yield:

: 1036-14-2
1-(4-methoxyphenylimino)methyl-2-naphthol

: 97095-06-2
1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid

Guidance literature:: Multi-step reaction with 2 steps

1: 38 percent / CH₂Cl₂; diethyl ether / 1.) 8 d, room temp.; 2.) 1 d, reflux

2: 59 percent / hydrochinone / toluene / 168 h / 110 - 120 °C

With hydroquinone; In diethyl ether; dichloromethane; toluene;
DOI:10.1002/jlac.198519850504

Reference yield:

: 104-94-9
4-methoxy-aniline

: 97095-06-2
1,4,4a,12c-Tetrahydro-N-(4-methoxyphenyl)-2,3-dimethyl-5-oxo-5H-6-oxabenzophenanthren-4a-carboxamid

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / molecular sieve / diethyl ether / 3 h / Ambient temperature

2: 38 percent / CH₂Cl₂; diethyl ether / 1.) 8 d, room temp.; 2.) 1 d, reflux

3: 59 percent / hydrochinone / toluene / 168 h / 110 - 120 °C

With molecular sieve; hydroquinone; In diethyl ether; dichloromethane; toluene;
DOI:10.1002/jlac.198519850504