4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

Base Information

Chemical Name:4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine
CAS No.:851908-78-6
Molecular Formula:C₃₈H₂₇N₅O₂
Molecular Weight:585.665
Hs Code.:

Synonyms:4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

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Chemical Property of 4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

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Technology Process of 4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

There total 4 articles about 4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 851908-77-5
2-[3-(4-hydroxyphenyl)-1-oxoprop-3-enyl]-6-[3-(4-methoxyphenyl)-1-oxoprop-3-enyl]pyridine

: 26482-00-8
1-(2-oxo-2-(2-pyridyl)ethyl)pyridinium iodide

: 851908-78-6
4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

Guidance literature:: With ammonium acetate; acetic acid; In methanol; Heating;
DOI:10.1039/b500209e

Reference yield:

: 851908-74-2
2-acetyl-6-[3-(4-hydroxyphenyl)-1-oxoprop-3-enyl]pyridine

: 851908-78-6
4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / Et₂NH / propan-1-ol / 2.5 h / Heating

2: 49 percent / NH₄OAc; AcOH / methanol / Heating

With ammonium acetate; acetic acid; diethylamine; In methanol; propan-1-ol; 2: Kroehnke reaction;
DOI:10.1039/b500209e

Reference yield:

: 1129-30-2
2,6-Diacetylpyridine

: 851908-78-6
4'-(4-hydroxyphenyl)-4'''-(4-methoxyphenyl)-2,2':6',2'':6'',2''':6''',2''''-quinquepyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 55 percent / Et₂NH / propan-1-ol / 2.5 h / Heating

2: 36 percent / Et₂NH / propan-1-ol / 2.5 h / Heating

3: 49 percent / NH₄OAc; AcOH / methanol / Heating

With ammonium acetate; acetic acid; diethylamine; In methanol; propan-1-ol; 3: Kroehnke reaction;
DOI:10.1039/b500209e