p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

Base Information

Chemical Name:p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt
CAS No.:73945-33-2
Molecular Formula:C₇H₈O₃S*C₂₇H₃₂N₄O₄S
Molecular Weight:680.846
Hs Code.:

Synonyms:p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

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Chemical Property of p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

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Technology Process of p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

There total 4 articles about p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 63502-90-9
p-amidinophenol p-toluenesulfonate

: 73945-36-5
4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

: 73945-33-2
p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; 1.) 0 deg C, 1 h, 2.) room temperature, 3 h;
DOI:10.1021/ja00529a053

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 73945-33-2
p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 3 steps

2: thionyl chloride, pyridine / Ambient temperature

3: 18 percent / triethylamine / dimethylformamide / 1.) 0 deg C, 1 h, 2.) room temperature, 3 h

With pyridine; thionyl chloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00529a053

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 73945-33-2
p-amidinophenyl trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylate p-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 3 steps

2: thionyl chloride, pyridine / Ambient temperature

3: 18 percent / triethylamine / dimethylformamide / 1.) 0 deg C, 1 h, 2.) room temperature, 3 h

With pyridine; thionyl chloride; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja00529a053