4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

Base Information

Chemical Name:4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride
CAS No.:73945-36-5
Molecular Formula:C₂₀H₂₅ClN₂O₃S*ClH
Molecular Weight:445.41
Hs Code.:

Synonyms:4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

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Chemical Property of 4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

Chemical Property:

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Technology Process of 4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

There total 3 articles about 4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73945-35-4
trans-N-(1-dimethylaminonaphthalene-5-sulfonyl)aminomethylcyclohexanecarboxylic acid

: 73945-36-5
4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

Guidance literature:: With pyridine; thionyl chloride; Ambient temperature;
DOI:10.1021/ja00529a053

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 73945-36-5
4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

2: thionyl chloride, pyridine / Ambient temperature

With pyridine; thionyl chloride;
DOI:10.1021/ja00529a053

Reference yield:

: 1197-18-8
trans-4-aminomethyl-cyclohexyl-carboxylic acid

: 73945-36-5
4-[(5-Dimethylamino-naphthalene-1-sulfonylamino)-methyl]-cyclohexanecarbonyl chloride; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

2: thionyl chloride, pyridine / Ambient temperature

With pyridine; thionyl chloride;
DOI:10.1021/ja00529a053