C₂₇H₄₀N₂O₅

Base Information

Chemical Name:C₂₇H₄₀N₂O₅
CAS No.:1292321-06-2
Molecular Formula:C₂₇H₄₀N₂O₅
Molecular Weight:472.625
Hs Code.:

C<sub>27</sub>H<sub>40</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₇H₄₀N₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₄₀N₂O₅

Chemical Property:

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Technology Process of C₂₇H₄₀N₂O₅

There total 8 articles about C₂₇H₄₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1194837-07-4
(S)-2-((1S,2S)-2-nitrocyclohexyl)butanoic acid:

: 1292321-02-8
(S,S,S)-hydrochloride*NH2-γ-(Et)ACHA-OBn

: 1292321-04-0
C₂₇H₄₀N₂O₅

: 1292321-06-2
C₂₇H₄₀N₂O₅

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

Reference yield:

: 2562-37-0
1-nitrocyclohexene

: 1292321-04-0
C₂₇H₄₀N₂O₅

: 1292321-06-2
C₂₇H₄₀N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: 3-nitrobenzoic acid; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine / dichloromethane / 0.02 h / 20 °C

1.2: 36 h / 23 °C

2.1: sodium tetrahydroborate; methanol / 0 °C

3.1: Jones reagent / acetone / 5 h / 0 - 20 °C

4.1: hydrogen / Raney nickel / methanol / 24 h / 2068.65 Torr / Inert atmosphere

5.1: chloro-trimethyl-silane / dichloromethane / 2 h / 20 °C

5.2: 12 h / 0 - 20 °C

6.1: caesium carbonate / N,N-dimethyl-formamide

7.1: hydrogenchloride / 1,4-dioxane

8.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide

With hydrogenchloride; methanol; sodium tetrahydroborate; Jones reagent; chloro-trimethyl-silane; hydrogen; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; 3-nitrobenzoic acid; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; 1.1: Michael Condensation / 1.2: Michael Condensation;

Reference yield:

: 1194837-06-3
(S)-2-((1S,2S)-2-nitrocyclohexyl)butan-1-ol

: 1292321-04-0
C₂₇H₄₀N₂O₅

: 1292321-06-2
C₂₇H₄₀N₂O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: Jones reagent / acetone / 5 h / 0 - 20 °C

2.1: hydrogen / Raney nickel / methanol / 24 h / 2068.65 Torr / Inert atmosphere

3.1: chloro-trimethyl-silane / dichloromethane / 2 h / 20 °C

3.2: 12 h / 0 - 20 °C

4.1: caesium carbonate / N,N-dimethyl-formamide

5.1: hydrogenchloride / 1,4-dioxane

6.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide

With hydrogenchloride; Jones reagent; chloro-trimethyl-silane; hydrogen; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; Raney nickel; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;