Cyclohexen-1-nitryl-6-oxo

Base Information

• Chemical Name: Cyclohexen-1-nitryl-6-oxo
• CAS No.: 91624-93-0
• Molecular Formula: C7H7 N O
• Molecular Weight: 121.139
• Mol file: 91624-93-0.mol

Synonyms:2-Cyano-2-cyclohexen-1-one;6-Oxo-1-cyclohexene-1-carbonitrile

Chemical Property of Cyclohexen-1-nitryl-6-oxo

Chemical Property:

• PSA: 40.86000
• LogP: 1.18938

Purity/Quality:

99% ^*data from raw suppliers

6-OXO-1-CYCLOHEXENE-1-CARBONITRILE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexen-1-nitryl-6-oxo

There total 3 articles about Cyclohexen-1-nitryl-6-oxo which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-cyanomethyl-6,7,8-trioxabicyclo<3.2.1>octane → 6-oxocyclohexene-1-carbonitrile (91624-93-0)

Guidance literature:

With dimethylsulfide; In dichloromethane; for 35h; Ambient temperature;

DOI:10.1021/jo9822885

Reference yield: 85.0%

cyclopent-1-enyl-acetonitrile (22734-04-9) → 6-oxocyclohexene-1-carbonitrile (91624-93-0)

Guidance literature:

cyclopent-1-enyl-acetonitrile; With ozone; In dichloromethane; at -78 ℃;

With dimethylsulfide; In dichloromethane; at 20 ℃; for 36h; Inert atmosphere;

DOI:10.15227/orgsyn.078.0254

Reference yield:

cyclohex-1-enecarbonitrile (1855-63-6) → 6-oxocyclohexene-1-carbonitrile (91624-93-0)

Guidance literature:

With chromium(VI) oxide; acetic acid;

upstream raw materials:

cyclohex-1-enecarbonitrile

cyclopent-1-enyl-acetonitrile

Downstream raw materials:

6-dimethylamino-cyclohex-1-enecarbonitrile

1-allyl-6-oxocyclolhex-2-enecarbonitrile

[2-(tert-butyldimethylsilyloxy)-6-(5-chloro-2-methylpent-2-yl)cyclohexen-1-yl]carbonitrile