1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol

Base Information

• Chemical Name: 1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol
• CAS No.: 1609472-08-3
• Molecular Formula: C₂₁H₂₈O₅
• Molecular Weight: 360.45
• Mol file: 1609472-08-3.mol

Synonyms:1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol

Chemical Property of 1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol

Chemical Property:

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Technology Process of 1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol

There total 1 articles about 1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Bromo-5-methoxybenzaldehyde diethyl acetal (139962-94-0) + 1-(4-methoxyphenyl)ethanone (100-06-1) → 1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol (1609472-08-3) + C19H22O4 (1609472-27-6)

Guidance literature:

2-Bromo-5-methoxybenzaldehyde diethyl acetal; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.75h; Inert atmosphere;

1-(4-methoxyphenyl)ethanone; In tetrahydrofuran; hexane; at -78 - 20 ℃; Overall yield = 88 %; Inert atmosphere;

DOI:10.1002/adsc.201300868

Reference yield: 70.0%

1-methylindole (603-76-9) + 1-(2-(diethoxymethyl)-4-methoxyphenyl)-1-(4-methoxyphenyl)ethanol (1609472-08-3) → 9-methoxy-11-(4-methoxyphenyl)-5,6-dimethyl-5H-benzo[b]carbazole (1609472-11-8)

Guidance literature:

With toluene-4-sulfonic acid; In acetonitrile; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1002/adsc.201300868

upstream raw materials:

2-Bromo-5-methoxybenzaldehyde diethyl acetal

1-(4-methoxyphenyl)ethanone

Downstream raw materials:

9-methoxy-11-(4-methoxyphenyl)-5,6-dimethyl-5H-benzo[b]carbazole