2-(4-Methoxyphenyl)-1H-phenanthro[9,10-d]imidazole

Base Information

Chemical Name:2-(4-Methoxyphenyl)-1H-phenanthro[9,10-d]imidazole
CAS No.:36939-52-3
Molecular Formula:C₂₂H₁₆N₂O
Molecular Weight:324.382
Hs Code.:
DSSTox Substance ID:DTXSID301229658
Nikkaji Number:J1.015.942C

Synonyms:2-(4-Methoxyphenyl)-1H-phenanthro[9,10-d]imidazole;DTXSID301229658;36939-52-3

Suppliers and Price of 2-(4-Methoxyphenyl)-1H-phenanthro[9,10-d]imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(4-Methoxyphenyl)-1H-phenanthro[9,10-d]imidazole

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:324.126263138
Heavy Atom Count:25
Complexity:461

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=NC3=C(N2)C4=CC=CC=C4C5=CC=CC=C53

Technology Process of 2-(4-Methoxyphenyl)-1H-phenanthro[9,10-d]imidazole

There total 4 articles about 2-(4-Methoxyphenyl)-1H-phenanthro[9,10-d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 123-11-5
4-methoxy-benzaldehyde

: 84-11-7
9,10-phenanthrenequinone

: 36939-52-3
2-(4-methoxyphenyl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: With ammonium acetate; acetic acid; for 0.166667h; Reflux; Green chemistry;
DOI:10.17344/acsi.2016.3111

Reference yield: 85.0%

: 84-11-7
9,10-phenanthrenequinone

: 105-13-5
4-Methoxybenzyl alcohol

: 36939-52-3
2-(4-methoxyphenyl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: 4-Methoxybenzyl alcohol; With C₃₀H₃₂Cl₂N₂O₃Ru₂; potassium hydroxide; In toluene; at 110 ℃; for 3h;

9,10-phenanthrenequinone; With ammonium acetate; acetic acid; In toluene; for 5h;
DOI:10.1039/C8OB02785D

Reference yield:

: 105-13-5
4-Methoxybenzyl alcohol

: 36939-52-3
2-(4-methoxyphenyl)-1H-phenanthro[9,10-d]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 1-methyl-2-ohenyl-1H-phenanthro<9,10-d>imidazole; 2,6-dimethylpyridine / acetonitrile / Electrolysis

2: ammonium acetate; sodium dihydrogenphosphate / ethanol / 6 h / 150 °C / Sealed tube

With 2,6-dimethylpyridine; sodium dihydrogenphosphate; ammonium acetate; 1-methyl-2-ohenyl-1H-phenanthro<9,10-d>imidazole; In ethanol; acetonitrile;
DOI:10.1021/ja410865z