Technology Process of methyl 3-methoxy-2,6-dimethylbenzoate
There total 6 articles about methyl 3-methoxy-2,6-dimethylbenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 16h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: nitric acid; sulfuric acid / nitromethane / 21 h / 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere
3.1: tin(II) chloride dihdyrate / ethanol / 2 h / 80 °C
3.2: pH 5
4.1: water; sodium nitrite; sulfuric acid / 0 - 120 °C
5.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere
With
tin(II) chloride dihdyrate; sulfuric acid; water; nitric acid; potassium carbonate; sodium nitrite;
In
nitromethane; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; sodium nitrite; sulfuric acid / 0 - 120 °C
2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C / Inert atmosphere
With
sulfuric acid; water; potassium carbonate; sodium nitrite;
In
N,N-dimethyl-formamide;
