5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

Base Information

Chemical Name:5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine
CAS No.:1237587-83-5
Molecular Formula:C₁₇H₁₄Cl₂F₃N₃O
Molecular Weight:404.219
Hs Code.:

Synonyms:5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

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Chemical Property of 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

Chemical Property:

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Technology Process of 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

There total 5 articles about 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1071927-10-0
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylaniline

: 1237587-83-5
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

Guidance literature:: 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylaniline; With hydrogenchloride; sodium nitrite; In water; at 0 ℃;

With hydrogenchloride; tin(ll) chloride; In water;

With sodium hydrogencarbonate; In water;

Reference yield:

: 31680-07-6
4-methyl-3-nitrobenzaldehyde

: 1237587-83-5
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1 h / 20 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 50 °C

2.2: 6 h / 20 °C

3.1: water; acetic acid; iron / ethanol / 1.25 h / 75 °C

4.1: hydrogenchloride / water / 0.33 h / 20 °C

4.2: 0.17 h / 0 °C

With hydrogenchloride; N-chloro-succinimide; hydroxylamine hydrochloride; water; sodium acetate; iron; acetic acid; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 5-hydroxyiminomethyl-2-methylnitrobenzene

: 1237587-83-5
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 50 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 1.25 h / 75 °C

3.1: hydrogenchloride / water / 0.33 h / 20 °C

3.2: 0.17 h / 0 °C

With hydrogenchloride; N-chloro-succinimide; water; iron; acetic acid; In ethanol; water; N,N-dimethyl-formamide;