N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide

Base Information

Chemical Name:N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide
CAS No.:1237587-21-1
Molecular Formula:C₂₀H₁₅Cl₂F₆N₃O₂
Molecular Weight:514.254
Hs Code.:

Synonyms:N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide

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Chemical Property of N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide

Chemical Property:

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Technology Process of N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide

There total 5 articles about N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 41463-83-6
3,3,3-trifluoropropanoyl chloride

: 1237587-83-5
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenylhydrazine

: 1237587-21-1
N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide

Guidance literature:: With pyridine; In ethyl acetate; at 0 - 20 ℃;

Reference yield:

: 31680-07-6
4-methyl-3-nitrobenzaldehyde

: 1237587-21-1
N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1 h / 20 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 50 °C

2.2: 6 h / 20 °C

3.1: water; acetic acid; iron / ethanol / 1.25 h / 75 °C

4.1: hydrogenchloride / water / 0.33 h / 20 °C

4.2: 0.17 h / 0 °C

5.1: pyridine / ethyl acetate / 4 h / 0 - 20 °C

With pyridine; hydrogenchloride; N-chloro-succinimide; hydroxylamine hydrochloride; water; sodium acetate; iron; acetic acid; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 5-hydroxyiminomethyl-2-methylnitrobenzene

: 1237587-21-1
N'-{5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylphenyl}-3,3,3-trifluoropropionohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 50 °C

1.2: 6 h / 20 °C

2.1: water; acetic acid; iron / ethanol / 1.25 h / 75 °C

3.1: hydrogenchloride / water / 0.33 h / 20 °C

3.2: 0.17 h / 0 °C

4.1: pyridine / ethyl acetate / 4 h / 0 - 20 °C

With pyridine; hydrogenchloride; N-chloro-succinimide; water; iron; acetic acid; In ethanol; water; ethyl acetate; N,N-dimethyl-formamide;