3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester

Base Information

• Chemical Name: 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester
• CAS No.: 178871-08-4
• Molecular Formula: C₂₅H₂₈ClNO₆S
• Molecular Weight: 506.019

Synonyms:3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester

Chemical Property of 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester

Chemical Property:

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Technology Process of 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester

There total 1 articles about 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-isopropenyl-azulene-1-carboxylic acid methyl ester (178870-67-2) → 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester (178871-08-4)

Guidance literature:

With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; tert-butyl alcohol; for 18h; Ambient temperature;

DOI:10.1016/0968-0896(96)00038-7

Reference yield: 96.0%

benzoic acid anhydride (93-97-0) + 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester (178871-08-4) → 6-(2-Benzoyloxy-1-hydroxy-1-methyl-ethyl)-3-[4-(4-chloro-benzenesulfonylamino)-butyl]-azulene-1-carboxylic acid methyl ester (178871-18-6)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran; for 2h; Ambient temperature;

DOI:10.1016/0968-0896(96)00038-7

Reference yield: 93.0%

acetone (67-64-1) + 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(1,2-dihydroxy-1-methyl-ethyl)-azulene-1-carboxylic acid methyl ester (178871-08-4) → 3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(2,2,4-trimethyl-[1,3]dioxolan-4-yl)-azulene-1-carboxylic acid methyl ester (178871-09-5)

Guidance literature:

With toluene-4-sulfonic acid; for 3h; Ambient temperature;

DOI:10.1016/0968-0896(96)00038-7

upstream raw materials:

3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-isopropenyl-azulene-1-carboxylic acid methyl ester

Downstream raw materials:

6-(2-Benzoyloxy-1-hydroxy-1-methyl-ethyl)-3-[4-(4-chloro-benzenesulfonylamino)-butyl]-azulene-1-carboxylic acid methyl ester

3-[4-(4-Chloro-benzenesulfonylamino)-butyl]-6-(2,2,4-trimethyl-[1,3]dioxolan-4-yl)-azulene-1-carboxylic acid methyl ester

1-[4-(4-chlorobenzenesulfonylamino)butyl]-6-(2-hydroxy-1-hydroxymethyl)ethylazulene

3-[4-(4-chlorobenzenesulfonylamino)butyl]-6-(2-hydroxy-1-hydroxymethyl)ethylazulene-1-carboxylic acid

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