(-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate

Base Information

Chemical Name:(-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate
CAS No.:1622998-49-5
Molecular Formula:C₂₅H₂₈ClNO₇
Molecular Weight:489.953
Hs Code.:

Synonyms:(-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate

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Chemical Property of (-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate

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Technology Process of (-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate

There total 9 articles about (-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 920112-99-8
((-)-trans-acetic acid-3-(3-acetyl-2-hydroxy-4,6-dimethoxyphenyl)-1-methylpyrrolidin-2-yl)methyl ester

: 609-65-4
o-chlorobenzoyl chloride

: 1622998-49-5
(-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate

Guidance literature:: With triethylamine; In dichloromethane; at -5 - 30 ℃; Inert atmosphere;

Reference yield:

: 117955-09-6
(±)-trans-[1-methyl-3-(2,4,6-trimethoxyphenyl)pyrrolidin-2-yl]methanol

: 1622998-49-5
(-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: Di-p-toluoyl-L-tartaric acid / ethanol / 75 - 78 °C

1.2: 0.5 h

2.1: acetic acid / 40 °C / Inert atmosphere

2.2: 25 - 70 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / -5 - 30 °C / Inert atmosphere

With Di-p-toluoyl-L-tartaric acid; acetic acid; triethylamine; In ethanol; dichloromethane;

Reference yield:

: 1254504-57-8,1622998-48-4
C₁₅H₂₃NO₄*C₁₈H₁₄O₈

: 1622998-49-5
(-)-trans-2-(2-(acetoxymethyl)-1-methylpyrrolidin-3-yl)-6-acetyl-3,5-dimethoxyphenyl-2-chlorobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / Isopropyl acetate / 0.5 h

2.1: acetic acid / 40 °C / Inert atmosphere

2.2: 25 - 70 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / -5 - 30 °C / Inert atmosphere

With acetic acid; triethylamine; sodium hydroxide; In dichloromethane; Isopropyl acetate;