3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride

Base Information

Chemical Name:3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride
CAS No.:1361319-30-3
Molecular Formula:C₁₃H₁₇F₃N₂O₂*ClH
Molecular Weight:326.746
Hs Code.:

Synonyms:3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride

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Chemical Property of 3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride

Chemical Property:

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Technology Process of 3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride

There total 5 articles about 3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361319-29-0
3-[(tert-butoxycarbonyl)amino]-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate

: 1361319-30-3
3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 60 ℃; for 2h;

Reference yield:

: 1361319-26-7
methyl 3-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-2-[3-(trifluoromethyl)phenyl]propanoate

: 1361319-30-3
3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: water; sodium tetrahydroborate / isopropyl alcohol

1.2: 80 °C / pH 5

2.1: sodium hydrogencarbonate / acetonitrile; water / 20 °C

3.1: dmap; pyridine / 20 - 50 °C

4.1: hydrogenchloride / 1,4-dioxane / 2 h / 60 °C

With pyridine; hydrogenchloride; dmap; sodium tetrahydroborate; water; sodium hydrogencarbonate; In 1,4-dioxane; water; isopropyl alcohol; acetonitrile;

Reference yield:

: 1361319-27-8
tert-butyl {3-hydroxy-2-[3-(trifluoromethyl)phenyl]propyl}carbamate

: 1361319-30-3
3-amino-2-[3-(trifluoromethyl)phenyl]propyl ethylcarbamate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; pyridine / 20 - 50 °C

2: hydrogenchloride / 1,4-dioxane / 2 h / 60 °C

With pyridine; hydrogenchloride; dmap; In 1,4-dioxane;