bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

Base Information

Chemical Name:bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron
CAS No.:32660-24-5
Molecular Formula:C₃₄H₂₈FeO₂P₂
Molecular Weight:586.39
Hs Code.:

Synonyms:bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

Suppliers and Price of bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

There total 7 articles about bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 7722-84-1
dihydrogen peroxide

: 32660-24-5
bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

Guidance literature:: In water; acetone; aq. H2O2 added to acetone soln. of (C5H4PPh2)2Fe under reflux; stirred overnight; filtered; washed with acetone, Et2O; air dried;
DOI:10.1016/j.poly.2009.02.028

Reference yield: 82.0%

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: 32660-24-5
bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

Guidance literature:: With dihydrogen peroxide; In water; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201201499

Reference yield: 78.0%

: [Cu2(μ-Cl)2(κ(2)-P,P-1,1'-bis(diphenylphosphino)ferrocene)2]

: 103-84-4
Acetanilid

: 32660-24-5
bis(2-(diphenylphosphoryl)cyclopenta-2,4-dien-1-yl)iron

Guidance literature:: With sodium methoxide; air; In dichloromethane; CH2Cl2 added to mixt. of Fe-Cu complex, acetanilide and NaOMe; stirred at room temp. in air for 24 h; filtered over Celite; solvent removed from filtrate by rotary evapn. at room temp.; dissolved in Et2O; crystd.; detd. by elem. anal. and X-ray crystallography;
DOI:10.1016/j.molstruc.2012.03.020