sodium triethylheptynylgallate

Base Information

• Chemical Name: sodium triethylheptynylgallate
• CAS No.: 80359-12-2
• Molecular Formula: C₁₃H₂₆Ga*Na
• Molecular Weight: 275.062

Synonyms:sodium triethylheptynylgallate

Chemical Property of sodium triethylheptynylgallate

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

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Technology Process of sodium triethylheptynylgallate

There total 1 articles about sodium triethylheptynylgallate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Na(1+)*(CH3CH2)3GaH(1-)=Na[(CH3CH2)3GaH] (64138-45-0) + 1-Heptyne (628-71-7) → hydrogen (1333-74-0) + sodium triethylheptynylgallate (80359-12-2)

Guidance literature:

In hexane; 4 d at 20°C (or eith excess of 1-heptyne at 60°C for 6 h); distilled off; elem. anal.;

DOI:10.1007/BF00963428

Reference yield: 95.0%

triethyloxonium fluoroborate (368-39-8) + sodium triethylheptynylgallate (80359-12-2) → ethane (74-84-0) + 3-nonyne (20184-89-8)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1007/BF00963428

Reference yield:

sodium triethylheptynylgallate (80359-12-2) → ethane (74-84-0) + 1-Heptyne (628-71-7)

Guidance literature:

With hydrogenchloride; In diethyl ether; at -50 ℃; Yields of byproduct given;

DOI:10.1007/BF00963428

upstream raw materials:

Na⁽¹⁺⁾*(CH₃CH₂)3GaH^(1-)=Na[(CH₃CH₂)3GaH]

1-Heptyne

Downstream raw materials:

3-nonyn-1-ol

ethane

3-nonyne

1-Heptyne

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