METHYL-3-(4-PYRIDYL)PROPANOATE

Base Information

• Chemical Name: METHYL-3-(4-PYRIDYL)PROPANOATE
• CAS No.: 90610-07-4
• Molecular Formula: C9H11 N O2
• Molecular Weight: 165.192
• Hs Code.: 2933399990
• Mol file: 90610-07-4.mol

Synonyms:4-Pyridinepropionicacid, methyl ester (6CI,7CI); Methyl 3-(4-pyridyl)propionate

Chemical Property of METHYL-3-(4-PYRIDYL)PROPANOATE

Chemical Property:

• Vapor Pressure: 0.0168mmHg at 25°C
• Refractive Index: 1.503
• Boiling Point: 254.9°Cat760mmHg
• Flash Point: 107.9°C
• PSA: 39.19000
• Density: 1.086g/cm³
• LogP: 1.18720

Purity/Quality:

97% ^*data from raw suppliers

Methyl3-(4-Pyridyl)propanoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL-3-(4-PYRIDYL)PROPANOATE

There total 9 articles about METHYL-3-(4-PYRIDYL)PROPANOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(E)-methyl-3-(pyridine-4-yl)prop-2-enoate (7340-34-3) → 4-pyridinepropanoic acid methyl ester (90610-07-4)

Guidance literature:

With palladium 10% on activated carbon; In methanol; at 20 ℃; for 4h;

DOI:10.1021/jm301247n

Reference yield: 98.0%

ethyl 3-(pyridin-4-yl)prop-2-enoate (24489-96-1) → 4-pyridinepropanoic acid methyl ester (90610-07-4)

Guidance literature:

With hydrazine hydrate; In acetonitrile; at 20 ℃; for 24h; Irradiation;

DOI:10.1002/ejoc.201403021

Reference yield: 61.0%

pyridine-4-carbonitrile (100-48-1) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → 4-pyridinepropanoic acid methyl ester (90610-07-4)

Guidance literature:

With bis(acetylacetonate)nickel(II); tetrabutylammonium perchlorate; sodium carbonate; In 1,2-dichloro-ethane; acetonitrile; at 50 ℃; for 3h;

DOI:10.1021/acs.orglett.0c01014

upstream raw materials:

methanol

3-pyridin-4-yl-propionic acid

(E)-methyl 3-(pyridine-4-yl)prop-2-enoate

4-bromopyridin

Downstream raw materials:

C₉H₁₂N₂O₂*C₉H₁₂O₃S

methyl-3-[2-n-butyl-1-(2-chlorophenyl)methyl-1H-imidazol-5-yl]-3-hydroxy-2-[(pyridin-4-yl)methyl]propanoate

3-pyridin-4-yl-propionic acid

(E)-3-[2-n-butyl-1-[(2-chlorophenyl)methyl}-1H-imidazol-5-yl]-2-(pyridin-4-yl)methyl-2-propenoic acid

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