(4-Bromo-3-methylphenyl)(methyl)sulphane

Base Information

• Chemical Name: (4-Bromo-3-methylphenyl)(methyl)sulphane
• CAS No.: 90532-02-8
• Molecular Formula: C8H9 Br S
• Molecular Weight: 217.129
• Hs Code.: 2930909090
• Mol file: 90532-02-8.mol

Synonyms:Sulfide,4-bromo-m-tolyl methyl (6CI,7CI); 1-Bromo-2-methyl-4-(methylsulfanyl)benzene;1-Bromo-2-methyl-4-(methylthio)benzene

Chemical Property of (4-Bromo-3-methylphenyl)(methyl)sulphane

Chemical Property:

• Vapor Pressure: 0.0269mmHg at 25°C
• Refractive Index: 1.608
• Boiling Point: 254.9°Cat760mmHg
• Flash Point: 108°C
• PSA: 25.30000
• Density: 1.45g/cm³
• LogP: 3.47940
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Bromo-3-methylthioanisole ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4-Bromo-3-methylphenyl)(methyl)sulphane

There total 8 articles about (4-Bromo-3-methylphenyl)(methyl)sulphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

3-methylthioanisole (4886-77-5) → 1-bromo-2-methyl-4-methylsulfanylbenzene (90532-02-8)

Guidance literature:

With bromine; acetic acid; at 0 - 20 ℃;

Reference yield: 76.0%

sodium thiomethanolate + 2-Bromo-5-fluorotoluene (452-63-1) → 1-bromo-2-methyl-4-methylsulfanylbenzene (90532-02-8)

Guidance literature:

In N,N-dimethyl-formamide; at 100 ℃; Inert atmosphere;

Reference yield:

3-methyl-4-bromothiophenol (14395-52-9) + methyl iodide (74-88-4) → 1-bromo-2-methyl-4-methylsulfanylbenzene (90532-02-8)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.25h;

upstream raw materials:

3-methylthioanisole

3-methyl-4-bromothiophenol

methyl iodide

2-Bromo-5-fluorotoluene

Downstream raw materials:

2-methyl-4-(methylsulfanyl)phenylboronic acid

2-methyl-4-(methylsulfinyl)phenyl bromide

(2-methyl-4-methylsulfanylphenyl)-acetic acid tert-butyl ester

N-Benzooxazol-2-yl-3-(4-fluoro-phenyl)-2-(4-methanesulfonyl-2-methyl-phenyl)-propionamide

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