hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)

Base Information

Chemical Name:hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)
CAS No.:1198174-23-0
Molecular Formula:C₃₀H₃₆N₃O₉P₃
Molecular Weight:675.552
Hs Code.:

Synonyms:hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)

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Chemical Property of hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)

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Technology Process of hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)

There total 3 articles about hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1169964-41-3
2,4,6-tris(4-(bromomethyl)phen-yl)-1,3,5-triazine

: 121-45-9
phosphorous acid trimethyl ester

: 1198174-23-0
hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)

Guidance literature:: for 5h; Reflux;
DOI:10.1002/cphc.201600280

Reference yield: 78.0%

: 6726-45-0
2,4,6-tris(p-tolyl)-1,3,5-triazine

: 121-45-9
phosphorous acid trimethyl ester

: 1198174-23-0
hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)

Guidance literature:: 2,4,6-tris(p-tolyl)-1,3,5-triazine; With N-Bromosuccinimide; dibenzoyl peroxide; In chlorobenzene; at 110 ℃; for 7h;

phosphorous acid trimethyl ester; for 9h; Reflux;
DOI:10.1007/s11426-013-4924-7

Reference yield:

: 6726-45-0
2,4,6-tris(p-tolyl)-1,3,5-triazine

: 1198174-23-0
hexamethyl (((1,3,5-triazine-2,4,6-triyl)tris(benzene-4,1-3-diyl))tris(methylene))tris(phosphonate)

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / chlorobenzene / 7 h / 110 °C

2: chlorobenzene / 9 h / Reflux

With N-Bromosuccinimide; dibenzoyl peroxide; In chlorobenzene;
DOI:10.1016/j.tetlet.2012.11.131